ISBN: 379851111x-c
TITLE: Structure Elucidation by Modern NMR
AUTHOR: Duddeck, Dietrich, Tth
TOC:

Foreword
1 Introduction 1
2 Methodology 7
2.1 High Magnetic Fields 8
2.2 One-Dimensional ^1H and ^13C NMR Spectra (INEPT, DEPT) 10
2.3 Two-Dimensional ^1H, ^1H Correlation (COSY, Linear Prediction, Pulsed Field Gradients, TOCSY) 15
2.4 Two-Dimensional ^13C, ^1H One-Bond Correlation (HETCOR, Inverse Detection, HSQC, HMQC, HMQC-TOCSY) 23
2.5 Two-Dimensional ^13C, ^1H Long-Range Correlation (COLOC, HMBC) 29
2.6 ^13C, ^13C-Correlation (INADEQUATE) 32
2.7 Dipolar Coupling Experiments (NOE difference, NOESY, ROESY) 35
2.8 Appendix: ^1H and ^13C NMR Data of Quinidine 42
3 Demonstration Examples 44
3.1 Formation of a Novel Benzothiazoline Derivative by Ring Contraction 44
3.2 Structure Elucidation of a Triterpene Saponin 54
4 Exercises 71
5 Strategies 161
6 Solutions 167
Explanation of Acronyms 203
Subject Index 204
Compound Index 206
END
