ISBN: 3540425989
TITLE: Microreaction Technology
AUTHOR: Matlosz et al. (Eds.)
TOC:

Author index XIII
Part 1
Keynote Lectures
Micro fabrication for process intensification 3
W. Ehrfeld, U. Ehrfeld
Microstructures for smart reactors: Precision perfomance in industrial production 13
M. Matlosz, S. Rode, J.-M. Commenge
Part 2
Design and Production of Microreactor Devices and Systems
Lecture Session
Microfluidics and microtechnology for microreactor systems 25
N.R. Tas, R.E. Oosterbroek, T.T. Veenstra, M. Elwenspoek, A. van den Berg
Micromachined straight-through silicon microchannel array for mono-dispersed microspheres 41
I. Kobayashi, M. Nakajima, Y. Kikuchi, K. Chun, H. Fujita
Development of a cooled microreactor for platinum catalyzed ammonia oxidation 49
E. V. Rebrov, M.H.J.M. de Croon, J.C. Schouten
Microchemical systems for direct fluorination of aromatics 60
N. de Mas, R.J. Jackman, M.A. Schmidt, K.F. Jensen
Design, fabrication and experimental study of new compact mini heat-exchangers 68
L. Luo, B. Hoareau, U. D'Ortona, D. Tondeur, H. Le Gall, S. Corbel
Poster Session
Development of a self-heating catalytic microreactor 70
K. Kusakabe, D. Miyagawa, Y. Gu, H. Maeda, S. Morooka
Preparation of microchannel palladium membranes by electrolysis 78
K. Kusakabe, M. Takahashi, H. Maeda, S. Morooka
Heating concepts for ceramic microreactors 86
R. Knitter, R. Lurk, M. Rohde, S. Stolz, V. Winter
Design and fabrication of zeolite-containing microstructures 94
Y.S.S. Wan, J.L.H.Chau, A. Gavriilidis, K.L.Yeung
New process for manufacturing ceramic microfluidic devices for microreactor and bioanalytical applications 103
C. Provin, S. Monneret, H. Le Gall, H. Rigneault, P.-F. Lenne, H. Giovannini
Macroscale production of microsystems 113
M. Schreiber, C.M. Hagg, U. Schubert, A.H. Whitehead
Part 3
Mathematical Modelling and Systems Analysis for Microreaction Technology and Bioanalytical Devices
Lecture Session
Prediction of the potential of microreactors for heterogeneously catalysed gas phase reactions 121
T. Stief, O.-U. Langer
Poster Session
Microchannel reactors for kinetic measurement: Influence of diffusion and dispersion on experimental accuracy 131
J.M. Commenge, L. Falk, J.P. Corriou, M. Matlosz
A vertically-averaged formulation of wall catalytic reactions in microchannel flows: single isothermal & non-isothermal reactions 141
D. Gobby, I. Eames, A. Gavriilidis
Part 4
Characterization of Microstructured Unit Operation and Reaction Modules
Lecture Session
Intensification in microstructured unit operations: Performance comparison between mega and microscale 153
A. R. Oroskar, K. M. VandenBussche, S. F. Abdo
A new microstructure device for fast temperature cycling for chemical reactions 164
J. Brandner, M. Fichtner, K. Schubert, M.A. Liauw, G. Emig
Photochemical reactions and online product detection, in microfabricated reactors 175
H. Lu, M.A. Schmidt, K.F. Jensen
Chaotic mixing in electrokinetically and pressure driven micro flows 185
Y.-K. Lee, J. Deval, P. Tabeling, C.-M. Ho
Filamentous catalytic beds for the design of a membrane microreactor: Propane dehydrogenation as a case study 192
O. Wolfrath, L. Kiwi-Minsker, A. Renken
Characterization of a gas/liquid microreactor, the micro bubble column: Determination of specific inter-facial area 202
V. Haverkamp, G. Emig, V. Hessel, M. Liauw, H. Lwe
Visualization of flow patterns and chemical synthesis in transparent Micromixers 215
T. Herweck, S. Hardt, V. Hessel, H. Lwe, C. Hofmann, F. Weise, T. Dietrich, A. Freitag
Forced periodic temperature oscillations in microchannel reactors 230
A. Rouge, A. Renken
Poster Session
Comparison of Ag/AI- and Ag/alpha-Ag_2O_3 catalytic surfaces for the partial oxidation of ethene in microchannel reactors 240
A. Kursawe, D. Hnicke
Monodispersed droplet formation caused by interfacial tension from microfabricated channel array 252
S. Sugiura, M. Nakajima, M. Seki
Investigation of microfluidics and heat transferability inside a microreactor array made of glass 262
E. Marioth, S. Loebbecke, M. Scholz, F. Schnrer, T. Trcke, J. Antes, H. H. Krause
Part 5
Application of Microdevices for Production, Energy and Transportation Systems
Lecture Session
Sub-watt power using an integrated fuel processor and fuel cell 277
E. Jones, J. Holladay, S. Perry, R. Orth, B. Rozmiarek, J. Hu, M. Phelps, C. Guzman
Catalytic microreactor systems for hydrogen generation 286
P.M. Irving, W. Lloyd Allen, T. Healey, Q. Ming, W.J. Thomson
Palladium based micro-membrane for water gas shift reaction and hydrogen gas separation 295
S. V. Karnik, M.K. Hatalis, M. V. Kothare
Demonstration of energy efficient steam reforming in microchannels for automotive fuel processing 303
G.A. Whyatt, W.E. TeGrotenhuis, J.G.H. Geeting, J.M. Davis, R.S. Wegeng, L.R. Pederson
A microstructure reactor system for the controlled oxidation of hydrogen for possible application in space 313
K. Haas-Santo, 0. Grke, K. Schubert, J. Fiedler, H. Funke
Poster Session
Catalyst coating in microreactors for methanol steam reforming: Kinetics 322
P. Reuse, P. Tribolet, L. Kiwi-Minsker, A. Renken
A microreactor for in-situ hydrogen production by catalytic methanol Reforming 332
A. V. Pattekar, M. V. Kothare, S. V. Kamik, M.K. Hatalis
Applications for micro chemical and thermal systems 343
D. L. Brenchley
Mixing simulation of a zigzag microchannel: A step towards the methoxylation of methyl-2-furoate 350
V. Mengeaud, R. Ferrigno, J. Josserand, H.H. Girault
Fuel processor development for a soldier-portable fuel cell system 359
D.R. Palo, J.D. Holladay, R.T. Rozmiarek, C.E. Guzman-Leong, Y. Wang, J. Hu, Y.-H. Chin, R.A. Dagle, E.G. Baker
MiRTH-e: Micro reactor technology for hydrogen and electricity 368
E. R. Delsman, E. V. Rebrov, M.H.J.M. de Croon, J.C. Schouten, G. J. Kramer, V. Cominos, T. Richter, T. T. Veenstra, A. van den Berg, P. D. Cobden, F.A. de Bruijn, C. Ferret, U. D'Ortona, L. Falk
Part 6
Microreactors as Tools in Chemical Research
Lecture Session
Microreactors as tools in chemical research 377
O. Woerz
Microchannel reactor for the partial oxidation of isoprene 387
S. Walter, E. Joannet, M. Schiel, I. Boullet, R. Philipps, M.A. Liauw
Selective oxidation of 1-butene to maleic anhydride - comparison of the performance between microchannel reactors and a fixed bed reactor 397
S. Kah, D. Hnicke
Application of a micromixer for the high throughput screening of fluid-liquid Molecular catalysis 408
C. de Bellefon, S. Caravieilhes, P. Grenouillet
A novel cross-flow microreactor for kinetic studies of catalytic processes 414
S. K. Ajmera, C. Delattre, M.A. Schmidt, K. F. Jensen
A new microreactor for the solution-phase synthesis of potential drugs 424
U. Kunz, A. Kirschning
Investigation, analysis and optimization of exothermic nitrations in Microreactor processes 446
J. Antes, T. Trcke, J. Kerth, E. Marioth, F. Schnrer, H.H. Krause, S. Lbbecke
Development of a microreactor for solid phase synthesis 455
E. Bremus-Kbberling, A. Gillner, M. Webner, U. Russek, J. Kbberling, D. Enders, S. Brandtner
Poster Session
Catalysts and reaction conditions screening by microreactor devices for exhaust gas purification 464
I.R. Tamas, R. Ganea, G. Pop
Liquid phase hydrogenation of p-nitrotoluene in microchannel reactors 470
R. Fdisch, D. Hnicke, Y. Xu, B. Platzer
Monitoring of chemical processes in microreactors by adapting FTIR Microscopy and HPLC 479
T. Trcke, W. Schweikert, F. Lechner, J. Antes, H.H. Krause, S. Lbbecke
Suitability of various types of micromixers for the forced precipitation of calcium carbonate 489
R. Schenk, M. Donnet, V. Hessel, C. Hofmann, N. Jongen, H. Lwe
Microdevice-based system for rapid catalyst development 499
R.S. Besser, X. Ouyang, J. Fort, H. Surangalikar
The synthesis of peptides using micro reactors 508
P. Watts, C. Wiles, S.J. Haswell, E. Pombo-Villar, P. Styring
Part 7
Analytical and Biological Applications
Lecture Session
BIOCHIPS: Lab-on-a-chip and DNA chips, new tools for high throughput genetic analysis and diagnostics 521
M. Cuzin, A. Fuchs, P. Caillat, Y. Fouillet
Fabrication of disposable plastic microplates with 98 integrated microfluidic capillary electroporesis (CE) structures for high throughput screening (HTS) 532
A.E. Guber, M. Heckele, D. Herrmann, A. Muslija, T. Schaller, A. Gerlach, G. Knebel
Diagnostic analyses by biochemical reactions and separations on a chip 542
M. Seki, J. W. Hong, R. Aoyama, R. Ezaki, Y. Kakigi, M. Yamada, T. Fujii, I. Endo
In situ and ex situ fabrication of DNA chips by microdeposition 552
M. Cabrera, M. Jaber, J.P. Cloarec, J.R. Martin, E. Souteryand, V. Dugas, J. Broutin, F. Bessueille, M. Bras, J.P. Chauvet
Poster Session
Chemical and biological sensors based on modified electrodes with Electropolymerized diamines 561
B. Lakard, G. Herlem, B. Fahys, M. de la Bachelerie, W. Daniau, G. Martin
A fluidic MEMS for protein identification by electrospray ionization/mass spectrometry 572
C. Druon, X. Mlique, C. Rolando, P. Tabourier
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